By J S Brimacombe
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(from preface)Volume forty seven of Advances in Heterocyciic Chemistry is, in contrast to such a lot volumes, a monograph and bargains with the quantitative elements of electro-philic substitution of heterocycles. it's written through Roger Taylor of the collage of Sussex, Brighton, England, and your editor with one bankruptcy contributed through Ross Grimmett of the college of Otago in New Zealand.
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Introductory cost £300 / €399 / $540, legitimate till December 31, 2016, thereafter £340 / €449 / $605This three-volume set represents the 1st finished insurance of the swiftly increasing box of Lewis base catalysis that has attracted huge, immense cognizance in recent times. Lewis base catalysis is a conceptually novel paradigm that encompasses a really big variety of preparatively worthy changes and is very potent for enantioselectively developing new stereogenic facilities.
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2-Esters (60) could also be prepared in high yield by reaction of methyl a-D-glucopyranoside with an equimolar proportion of dibutyltin oxide in methanol, to yield the 2,3-O-dibutylstannylene derivative (59), and then with an acid chloride in the presence of triethylamine (Scheme 19). Other examples of / OH OH / BU, (59) Reagents: i, Bu,SnO-MeOH; ii, RCOCl-Et3N Scheme 19 19* R. M. Munavu and H. H. Szmant, J. Org. , 1976,41, 1832. 202 Similarly, the 0 II RCH,OCK R C H, OSn Bu (63) “CMe, Reagents: i, NBS-CCl,; ii, PhCHO-NBS-CCI, Scheme 20 reaction of 1,2:5,6-di-O-isopropylidene-3-O-tributylstannyl-~-~-glucofuranose with NBS and n-hexanal furnished the corresponding 3-hexanoate in high yield.
Akad. , Ser. , 1975, 1843 (Chem. , 1976, 84, 31 3192). L. L. Danilov, L. V. Volkova, and R. P. Evstigneeva, Zhur. ,1975, 45, 2307 (Chem. , 1976, 84, 105 919n). L. L. Danilov, L. V. Volkova, V. A. Bondarenko, and R. P. Evstigneeva, Bioorg. , 1975, 1, 905 (Chem. , 1976, 84, 105 921p). M. A. Grum-Grzhimailo, L. V. Volkova, and R. P. Evstigneeva, Zhur. , 1976, 46, 1386 (Chem. A h , 1976, 85, 143 372p). P. F. Blackmore, J. F. Williams, and J . K. S. Letters, 1976, 64, 222. N. K. Kochetkov, E. E. Nifant’ev, M.
E. Pfeffer, E. S. Rothman, and G. G. Moore, J. Org. , 1976, 41, 2925. T. D. Audichya, IndinnJ. , 1976, 14B, 111 (Chem. , 1976, 85, 177 809b). S. Ando, T. Ariga, and T. Yamakawa, Bull. Chem. Japan, 1976, 49, 1335. J. G. Buchanan and A. R. , 1976, 49, 289. H. Paulsen, H. Hohne, and P. L. Durette, Chem. , 1976, 109, 597. H. Paulsen and R. Dammeyer, Chem. , 1976, 109, 1837. ~~ The conversion of adenosine into a 2’,3’-O-alkoxymethylene derivative is noted in Chapter 21,224and the formation of the thio-orthoester (24) from methyl (1 ,2,3,4-tetra- O-acetyl- a - ~ - gucopyranosy1)uronate l is mentioned in Chapter 3.